Chemical Separations: Principles, Techniques and Experiments

SEPARATIONS INVOLVING PHASE CHANGES.

Volatilization.

Zone Melting.

Distillation: General Information.

Azeotropic and Extractive Distillations.

Steam and Immiscible Solvents Distillation.

Vacuum Distillation.

Molecular Distillation and Sublimation.

Lyophilization (Freeze Drying).

SEPARATIONS INVOLVING EXTRACTION.

Extraction: General Concepts.

Continuous Extraction.

Countercurrent (Extraction) Chromatography: The Ito Coil-Planet Centrifugal Extractor.

Solid Phase Extraction.

Supercritical Fluid Extraction.

SEPARATIONS INVOLVING CHROMATOGRAPHY.

Chromatography: General Theory.

Displacement and Multiple Column Partition Chromatography.

Affinity Chromatography.

Size Exclusion Chromatography (Gel Filtration;
Gel Permeation).

Flash Chromatography.

High Performance Liquid Chromatography (HPLC).

Gas-Liquid Chromatography.

Paper Chromatography.

Thin Layer Chromatography.

SEPARATIONS INVOLVING ION EXCHANGE RESINS.

Ion Exchange.

Ion Chromatography.

Ion Retardation, Ion Exclusion, and Ligand Exchange.

SEPARATIONS INVOLVING ELECTRIC FIELDS.

Electrodeposition.

Electrophoresis--General.

Immunoelectrophoresis.

Polyacrylamide Gel Disc Electrophoresis.

Ion Focusing, SDS, and Two-Dimensional Electrophoresis.

Capillary Zone Electrophoresis.

Field Flow Fractionation.

SEPARATIONS INVOLVING FLOTATION.

Purge and Trap and Dynamic Headspace Analysis

Foam Fractionation, Gas-, and Liquid-Assisted Flotation.

SEPARATIONS INVOLVING MEMBRANES.

Osmosis and Reverse Osmosis.

Dialysis and Electrodialysis

Filtering and Sieving.

SEPARATIONS INVOLVING MISCELLANEOUS TECHNIQUES.

Density Gradients.

Centrifugation.

Masking and Sequestering Agents.

Solubility.

Gas Analysis by Portable Orsat.

Appendices.

Index.